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        格氏試劑是由法國化學家維克多•格林尼亞(Victor Grignard)發(fā)現(xiàn)的含鹵化鎂的有機金屬化合物。由于其含有C-MgX基團,極易轉化成碳負離子,可通過烷基化、羰基加成、共軛加成等反應增長碳鏈;可實現(xiàn)官能團的轉化和多種含官能團有機化合物的合成;可通過轉金屬反應制備其它有機金屬化合物;還可以脫去亞胺的α-氫,用于α-烷基醛的合成反應。

近幾年,新型催化劑的使用及新合成方法的研究中,格氏試劑還可發(fā)生諸如偶聯(lián)、聚合、不對稱合成等反應,如:

(1) Fe催化下伯烷基格氏試劑與烯基或芳基羧化物的交叉
J. Am. Chem. Soc., 2009, 131 (41), 14656–14657
(2) 格氏試劑參與C-H活化的氯代噻吩均聚反應:

 

                                                                                                                     J.Am.Chem.Soc.,2011,133(25),9700–9703

(3) Ni催化下的烷基格氏試劑與烷基鹵化物的Alkyl-Alkyl Kumada交叉偶聯(lián)反應:

 

                                                                                                            J. Am. Chem. Soc., 2011, 133 (18), 7084–7095

(4) 芳基格氏試劑與烯烴的偶聯(lián)反應:

                                                                                                           J. Am. Chem. Soc., 2011, 133 (20), 7672–7675

(5) Cu催化劑催化下的Asymmetric Allylic Alkylation反應:

                                                                                                             J. Am. Chem. Soc., 2012, 134 (9), 4108–4111

★ 產品特點:
種類規(guī)格多
110多個品種,涵蓋脂肪烴及芳香烴格氏試劑,可最大化滿足科研和生產的需求;
反應收率高
大部分產品溶劑為通用無水THF,通過多項嚴格檢測,可有效提高反應收率;
可多次抽取
包裝設計獨特,多層密封襯墊,JKSeal 七孔可抽取式包裝,可有效延長保存時間;
成本優(yōu)勢好
極具競爭力的價格,同比進口產品價格低50%,90%以上的產品國內現(xiàn)貨供應充足,可提供多種規(guī)格鋼瓶大包裝。

R-MgBr 類格氏試劑

產品名稱
產品編號
CAS
產品規(guī)格
Allylmagnesium bromide, 1.0 M solution in diethyl ether, J&KSeal
烯丙基溴化鎂
100 mL
800 mL
2-Biphenylmagnesium bromide, 0.5 M solution in diethyl ether, J&KSeal
2-聯(lián)苯基溴化鎂
50 mL
500 mL
3-Biphenylmagnesium bromide, 0.5 M solution in THF, J&KSeal
3-聯(lián)苯基溴化鎂
50 mL
500 mL
4-Biphenylmagnesium bromide, 0.5 M solution in THF, J&KSeal
4-聯(lián)苯基溴化鎂
50 mL
500 mL
3,5-Bis(trifluoromethyl)phenylmagnesium bromide, 0.5 M solution in THF, J&KSeal
3,5-雙(三氟甲基)苯基溴化鎂
 
100 mL
500 mL
800 mL
3-Butenylmagnesium bromide, 0.5 M solution in THF, J&KSeal
3-丁烯基溴化鎂
 
100 mL
sec-Butylmagnesium bromide, 1.0 M solution in THF, J&KSeal
仲丁基溴化鎂
 
100 mL
500 mL
800 mL
4-tert-Butylphenylmagnesium bromide, 0.5 M solution in THF, J&KSeal
4-叔丁基苯基溴化鎂
 
100 mL
500 mL
800 mL
4-tert-Butylphenylmagnesium bromide, 2.0 M solution in diethyl ether, J&KSeal
4-叔丁基苯基溴化鎂
 
100 mL
500 mL
800 mL
4-Chlorophenylmagnesium bromide, 1.0 M solution in diethyl ether, J&KSeal
4-氯苯基溴化鎂
 
100 mL
500 mL
800 mL
5-Chloro-2-thienylmagnesium bromide, 0.5 M slurry in THF, J&KSeal
5-氯-2-噻吩基溴化鎂
 
50 mL
500 mL
Cyclohexylmagnesium bromide, 1.0 M solution in THF, J&KSeal
環(huán)己基溴化鎂
 
100 mL
500 mL
800 mL
 (Cyclohexylmethyl)magnesium bromide, 0.5 M solution in THF, J&KSeal
(環(huán)己基甲基)溴化鎂
 
100 mL
500 mL
Cyclopentylmagnesium bromide, 2.0 M solution in diethyl ether, J&KSeal
環(huán)戊基溴化鎂
 
100 mL
500 mL
800 mL
Cyclopropylmagnesium bromide, 0.5 M solution in THF, J&KSeal
環(huán)丙基溴化鎂
 
100 mL
500 mL
Decylmagnesium bromide, 1.0 M solution in diethyl ether, J&KSeal
癸基溴化鎂
 
100 mL
500 mL
800 mL
3,4-Difluorophenylmagnesium bromide, 0.5 M solution in THF, J&KSeal
3,4-二氟苯基溴化鎂
 
100 mL
3,5-Difluorophenylmagnesium bromide, 0.5 M solution in THF, J&KSeal
3,5-二氟苯基溴化鎂
 
100 mL
500 mL
3,4-Dimethoxyphenylmagnesium bromide, 0.5 M solution in THF, J&KSeal
3,4-二甲氧基苯基溴化鎂
 
50 mL
500 mL
2,5-Dimethylphenylmagnesium bromide, 1.0 M solution in THF, J&KSeal
2,5-二甲基苯基溴化鎂
 
100 mL
500 mL
800 mL
Dodecylmagnesium bromide, 1.0 M solution in diethyl ether, J&KSeal
十二烷基溴化鎂
100 mL
500 mL
800 mL
 (2-Ethylhexyl)magnesium bromide, 1.0 M solution in diethyl ether, J&KSeal
(2-乙基己基)溴化鎂
100 mL
500 mL
800 mL
Ethylmagnesium bromide, 3.0 M solution in diethyl ether, J&KSeal
乙基溴化鎂
100 mL
500 mL
800 mL
Ethylmagnesium bromide, 1.0 M solution in THF, J&KSeal
乙基溴化鎂
 
100 mL
500 mL
800 mL
Ethylmagnesium bromide, 1.0 M solution in tert-butyl methyl ether, J&KSeal
乙基溴化鎂
 
100 mL
500 mL
800 mL
Ethylmagnesium bromide, 3.4 M solution in 2-methyltetrahydrofuran, J&KSeal
乙基溴化鎂
 
100 mL
500 mL
800 mL
4-Ethylphenylmagnesium bromide, 0.5 M solution in THF, J&KSeal
4-乙基苯基溴化鎂
 
50 mL
500 mL
Ethynylmagnesium bromide, 0.5 M solution in THF, J&KSeal
乙炔基溴化鎂
 
100 mL
500 mL
800 mL
4-Fluoro-3-methylphenylmagnesium bromide, 1.0 M solution in THF, J&KSeal
4-氟-3-甲苯基溴化鎂
 
100 mL
500 mL
800 mL
3-Fluorophenylmagnesium bromide, 0.5 M solution in THF, J&KSeal
3-氟苯基溴化鎂
 
100 mL
500 mL
800 mL
3-Fluorophenylmagnesium bromide, 1.0 M solution in THF, J&KSeal
3-氟苯基溴化鎂
 
100 mL
500 mL
4-Fluorophenylmagnesium bromide, 2.0 M solution in diethyl ether, J&KSeal
4-氟苯基溴化鎂
 
100 mL
500 mL
800 mL
4-Fluorophenylmagnesium bromide, 0.8 M solution in THF, J&KSeal
4-氟苯基溴化鎂
 
100 mL
500 mL
Heptylmagnesium bromide solution, 1.0 M solution in diethyl ether, J&KSeal
庚基溴化鎂
 
100 mL
500 mL
Hexylmagnesium bromide, 0.8 M in THF, J&KSeal
己烷溴化鎂
 
100 mL
500 mL
800 mL
Isobutylmagnesium bromide, 2.0 M solution in diethyl ether, J&KSeal
異丁基溴化鎂
100 mL
500 mL
800 mL
Isopropylmagnesium bromide, 3.0 M in 2-Methyltetrahydrofuran, J&KSeal
異丙基溴化鎂
100 mL
500 mL
800 mL
Isopropylmagnesium bromide, 1.0 M solution in THF, J&KSeal
異丙基溴化鎂
100 mL
800 mL
2-Methoxyphenylmagnesium bromide, 1.0 M in THF, J&KSeal
2-甲氧基苯基溴化鎂
100 mL
500 mL
800 mL
2-Methoxyphenylmagnesium bromide, 1.0 M solution in diethyl ether, J&KSeal
2-甲氧基苯基溴化鎂
100 mL
500 mL
3-Methoxyphenylmagnesium bromide, 1M in THF/toluene (38/62), J&KSeal
3-甲氧苯基溴化鎂
100 mL
500 mL
800 mL
3-Methoxyphenylmagnesium bromide, 1.0 M solution in THF, J&KSeal
3-甲氧苯基溴化鎂
100 mL
500 mL
800 mL
4-Methoxyphenylmagnesium bromide, 1.0 M solution in THF, J&KSeal
4-甲氧基苯基溴化鎂
100 mL
500 mL
800 mL
4-Methoxyphenylmagnesium bromide, 0.5 M solution in THF, J&KSeal
4-甲氧基苯基溴化鎂
100 mL
500 mL
800 mL
3,4-(Methylenedioxy)phenylmagnesium bromide
1.0 M solution in THF: toluene (1:1), J&KSeal
3,4-(亞甲二氧基)苯基溴化鎂
100 mL
500 mL
800 mL
Methylmagnesium bromide, 1.0 M solution in dibutyl ether, J&KSeal
甲基溴化鎂
100 mL
500 mL
800 mL
Methylmagnesium bromide, 1.4 M in toluene/THF, J&KSeal
甲基溴化鎂
100 mL
800 mL
Methylmagnesium bromide, 3.0 M in 2-methyl-THF, J&KSeal
甲基溴化鎂
100 mL
800 mL
Methylmagnesium bromide, 3.0 M solution in diethyl ether, J&KSeal
甲基溴化鎂
100 mL
500 mL
800 mL
Methylmagnesium bromide, 1.0 M solution in THF, J&KSeal
甲基溴化鎂
100 mL
800 mL
1-Methyl-1-propenylmagnesium bromide, 0.5 M solution in THF, J&KSeal
1-甲基-1-丙烯基溴化鎂
100 mL
500 mL
800 mL
2-Methyl-1-propenylmagnesium bromide, 0.5 M solution in THF, J&KSeal
2-甲基-1-丙烯基溴化鎂
100 mL
500 mL
800 mL
3-Methyl-2-thienylmagnesium bromide, 0.5 M solution in THF, J&KSeal
3-甲基-2-噻吩基溴化鎂
50 mL
1-Naphthylmagnesium bromide, 0.25 M solution slurry in THF, J&KSeal
1-萘基溴化鎂
100 mL
500 mL
2-Naphthylmagnesium bromide, 0.5 M solution in THF, J&KSeal
2-萘基溴化鎂
100 mL
500 mL
Octylmagnesium bromide, 2.0 M in diethyl ether, J&KSeal
辛基溴化鎂
100 mL
500 mL
800 mL
Pentamethylenebis(magnesium bromide), 0.5 M solution in THF, J&KSeal
五亞甲基雙溴化鎂
100 mL
500 mL
800 mL
Pentylmagnesium bromide, 2.0 M solution in diethyl ether, J&KSeal
戊基溴化鎂
100 mL
500 mL
800 mL
Pentylmagnesium bromide, 1.0 M solution in THF, J&KSeal
戊基溴化鎂
100 mL
500 mL
800 mL
3-Pentylmagnesium bromide, 2.0 M solution in diethyl ether, J&KSeal
3-戊烷溴化鎂
100 mL
500 mL
Phenylmagnesium bromide, 2.9 M solution in 2-methyltetrahydrofuran, J&KSeal
苯基溴化鎂
100 mL
500 mL
800 mL
苯基溴化鎂
Phenylmagnesium bromide, 2.8 M solution in diethyl ether, J&KSeal
100 mL
500 mL
800 mL
Phenylmagnesium bromide, 1.0 M solution in THF, J&KSeal
苯基溴化鎂
100 mL
800 mL
Propylmagnesium bromide, 2.0 M solution in THF, J&KSeal
丙基溴化鎂
100 mL
800 mL
2-Thienylmagnesium bromide, 1.0 M solution in THF, J&KSeal
2-噻吩基溴化鎂
50 mL
4-Thioanisolemagnesium bromide, 0.5 M solution in THF, J&KSeal
4-硫代苯甲醚溴化鎂
100 mL
500 mL
o-Tolylmagnesium bromide, 2.0 M solution in diethyl ether, J&KSeal
鄰甲苯基溴化鎂
100 mL
500 mL
800 mL
p-Tolylmagnesium bromide, 0.5 M solution in diethyl ether, J&KSeal
對甲苯基溴化鎂
100 mL
500 mL
800 mL
p-Tolylmagnesium bromide, 1.0 M solution in THF, J&KSeal
對甲苯基溴化鎂
100 mL
500 mL
800 mL
2,4,6-Triisopropylphenylmagnesium bromide, 0.5 M solution in THF, J&KSeal
2,4,6-三異丙基苯基溴化鎂
N/A
100 mL
500 mL
Vinylmagnesium bromide, 1.0 M solution in THF, J&KSeal
乙烯基溴化鎂
100 mL
800 mL

R-MgCl 格氏試劑

產品名稱
產品編號
CAS
產品規(guī)格
Allylmagnesium chloride, 2.0 M solution in THF, J&KSeal
烯丙基氯化鎂
100 mL
500 mL
800 mL
10 L
Benzylmagnesium chloride, 1.0 M solution in diethyl ether, J&KSeal
芐基氯化鎂
100 mL
500 mL
800 mL
Benzylmagnesium chloride, 1.4 M solution in THF, J&KSeal
芐基氯化鎂
 
100 mL
800 mL
2-Butenylmagnesium chloride, 0.5 M solution in THF, J&KSeal
2-丁烯基氯化鎂
100 mL
n-Butylmagnesium chloride, 2.0 M solution in diethyl ether, J&KSeal
正丁基氯化鎂
100 mL
500 mL
800 mL
n-Butylmagnesium chloride, 2.0 M solution in THF, J&KSeal
正丁基氯化鎂
100 mL
800 mL
tert-Butylmagnesium chloride, 2.0 M solution in diethyl ether, J&KSeal
叔丁基氯化鎂
100 mL
500 mL
800 mL
tert-Butylmagnesium chloride, 1.0 M solution in THF, J&KSeal
叔丁基氯化鎂
100 mL
500 mL
800 mL
10 L
Cyclohexylmagnesium chloride, 2.0 M solution in diethyl ether, J&KSeal
環(huán)己基氯化鎂
100 mL
500 mL
800 mL
Cyclohexylmagnesium chloride, 1.3 M solution in THF/toluene (62/38), J&KSeal
環(huán)己基氯化鎂
100 mL
500 mL
800 mL
Cyclopentylmagnesium chloride, 2.0 M solution in diethyl ether, J&KSeal
環(huán)戊基氯化鎂
100 mL
500 mL
800 mL
Ethylmagnesium chloride, 2.0 M solution in THF, J&KSeal
乙基氯化鎂
100 mL
500 mL
800 mL
Ethynylmagnesium chloride, 0.5 M solution in THF, J&KSeal
乙炔基氯化鎂
100 mL
800 mL
4-Fluorobenzylmagnesium chloride, 0.25 M solution in diethyl ether, J&KSeal
4-氟苯基氯化鎂
100 mL
500 mL
Hexylmagnesium chloride, 1.8 M solution in THF, J&KSeal
己烷氯化鎂
100 mL
500 mL
800 mL
Isobutylmagnesium chloride, 2.0 M solution in THF, J&KSeal
異丁基氯化鎂
100 mL
500 mL
800 mL
Isobutylmagnesium chloride, 2.0 M solution in diethyl ether, J&KSeal
異丁基氯化鎂
100 mL
500 mL
800 mL
Isopropylmagnesium chloride, 2.0 M solution in diethyl ether, J&KSeal
異丙基氯化鎂
100 mL
500 mL
800 mL
Isopropylmagnesium chloride, 1.4 M solution in butyl diglyme, J&KSeal
異丙基氯化鎂
100 mL
500 mL
800 mL
Isopropylmagnesium chloride, 2.0 M solution in THF, J&KSeal
異丙基氯化鎂
100 mL
500 mL
800 mL
10 L
Isopropylmagnesium chloride-lithium chloride complex, 1.3 M solution in THF, J&KSeal
異丙基氯化鎂-氯化鋰
100 mL
500 mL
800 mL
2-Methylallylmagnesium chloride, 0.5 M solution in THF, J&KSeal
2-甲基烯丙基氯化鎂
100 mL
4-Methoxybenzylmagnesium chloride, 0.25 M solution in THF, J&KSeal
4-甲氧基苯甲基氯化鎂
100 mL
500 mL
Methylmagnesium chloride, 3.0 M solution in THF, J&KSeal
甲基氯化鎂
100 mL
800 mL
1-Methyl-2-propenylmagnesium chloride, 0.5 M solution in THF, J&KSeal
1-甲基-2-丙烯基氯化鎂
100 mL
500 mL
800 mL
Octadecylmagnesium chloride, 0.5 M solution in THF, J&KSeal
十八烷基氯化鎂
100 mL
500 mL
800 mL
Octylmagnesium chloride, 2.0 M solution in THF, J&KSeal
辛基氯化鎂
100 mL
500 mL
800 mL
Pentylmagnesium chloride, 2.0 M solution in THF, J&KSeal
戊烷氯化鎂
100 mL
500 mL
800 mL
Phenethylmagnesium chloride, 1.0 M solution in THF, J&KSeal
苯乙基氯化鎂
100 mL
500 mL
800 mL
Phenylmagnesium chloride, 2.0 M solution in THF, J&KSeal
苯基氯化鎂
100 mL
500 mL
800 mL
Propylmagnesium chloride, 2.0 M solution in diethyl ether, J&KSeal
丙基氯化鎂
100 mL
500 mL
800 mL
Tetradecylmagnesium chloride, 1.0 M solution in THF, J&KSeal
十四烷基氯化鎂
100 mL
500 mL
800 mL
 (Trimethylsilyl)methylmagnesium chloride, 1.0 M solution in diethyl ether, J&KSeal
(三甲基硅基)甲基氯化鎂
100 mL
500 mL
800 mL
Trimethylsilylmethylmagnesium chloride, 1.3 M solution in THF, J&KSeal
(三甲基硅基)甲基氯化鎂
100 mL
800 mL
o-Tolylmagnesium chloride, 1.4 M solution in THF/toluene(82/18),
J&KSeal
鄰甲苯基氯化鎂
100 mL
500 mL
800 mL
o-Tolylmagnesium chloride, 1.0 M solution in THF, J&KSeal
鄰甲苯基氯化鎂
100 mL
500 mL
800 mL

R-MgI 格氏試劑

產品名稱
產品編號
CAS
產品規(guī)格
Methylmagnesium iodide,3.0 M in diethyl ether, J&KSeal
甲基碘化鎂
100 mL
500 mL
800 mL

 

配套合成試劑
正丁基鋰
超干溶劑
水含量低至10 ppm
——最大程度地滿足苛刻的無水合成環(huán)境;
使用前無需再經過任何無水處理
——可直接用于對空氣及水分極其敏感的反應中;
抽取式包裝,含分子篩及不含分子篩兩類產品

——更多規(guī)格,更多選擇,適合不同類型實驗需求

百靈威超干溶劑,現(xiàn)貨充足,可提供多種規(guī)格大包裝,滿足不同反應投料量需求,試劑與大包裝質量標準統(tǒng)一,從此不必再為除去溶劑中微量水分而困擾,讓您的實驗變得更加簡單、安全、便捷!

★含分子篩類產品——特別添加分子篩,吸收微量水分,時時動態(tài)干燥。

產品名稱
純度
產品編號
CAS
Acetonitrile
乙腈
99.9%, water ≤ 50 ppm
Chlorobenzene
氯苯
99.8%, water ≤ 50 ppm
Dichloromethane
二氯甲烷
99.9%, water ≤ 30 ppm
1,2-Dichloroethane
1,2-二氯乙烷
99.5%, water ≤ 30 ppm
N,N-Dimethylacetamide
N,N-二甲基乙酰胺
99.8%, stabilized with 250 ppm BHT, water ≤ 50 ppm
N,N-Dimethylformamide
N,N-二甲基甲酰胺
99.8%, water ≤ 50 ppm
Dimethyl sulfoxide
二甲基亞砜
99.7%, water ≤ 50 ppm
1,4-Dioxane
1,4-二氧六環(huán)
99.5%, stabilized with BHT, water ≤ 50 ppm
Ethanol
乙醇
99.5%, water ≤ 50 ppm
Ethyl acetate
乙酸乙酯
99.9%, water ≤ 50 ppm
n-Heptane
正庚烷
99%, water ≤ 10 ppm
n-Hexane
正己烷
97.5%, water ≤ 50 ppm
Isopropanol
異丙醇
99.5%, water ≤ 50 ppm
Methanol
甲醇
99.9%, water ≤ 30 ppm
Methyl tert-butyl ether
甲基叔丁基醚
99%, water ≤ 30 ppm
Pyridine
吡啶
99.5%, water ≤ 50 ppm
Tetrahydrofuran
四氫呋喃
99.5%, stabilized with 250 ppm BHT, water ≤ 50 ppm

★不含分子篩類產品

品種多,規(guī)格全,更適合批量投料使用。

產品名稱
純度
產品編號
CAS
Acetone
丙酮
99.8%, water ≤ 50 ppm
Acetonitrile
乙腈
99.9%, water ≤ 30 ppm
Acetonitrile
乙腈
99.9% water ≤ 10 ppm
Anisole
苯甲醚
99.7%, water ≤ 20 ppm
Benzonitrile
芐腈
99%, water ≤ 30 ppm
Benzotrifluoride
三氟甲基苯
99%, water ≤ 10 ppm
Benzyl alcohol
芐醇
99%, water ≤ 30 ppm
1-Butanol
1-丁醇
99.5%, water ≤ 50 ppm
2-Butanol
2-丁醇
99.5%, water ≤ 50 ppm
Butyl acetate
乙酸正丁酯
99%, water ≤ 50 ppm
Butyl ether
正丁醚
99%, water ≤ 50 ppm
Chlorobenzene
氯苯
99.8%, water ≤ 50 ppm
1-Chlorobutane
1-氯丁烷
99.5%, water ≤ 20 ppm
Chloroform
氯仿
99.9%, water ≤ 30 ppm
Cyclohexane
環(huán)己烷
99.5%, water ≤ 10 ppm
Cyclopentane
環(huán)戊烷
98%, water ≤ 50 ppm
Decahydronaphthalene
十氫化萘
99%, water ≤ 20 ppm
1,2-Dichlorobenzene
1,2-二氯苯
99%, water ≤ 50 ppm
1,2-Dichloroethane
1,2-二氯乙烷
99.5%, water ≤ 30 ppm
Dichloromethane
二氯甲烷
99.9%, stabilized with amylene, water ≤ 30 ppm
Diethylene glycol dimethyl ether
二乙二醇二甲醚
99.5%, water ≤ 50 ppm
1,2-Dimethoxyethane
1,2-二甲氧基乙烷
99.5%, water ≤ 30 ppm
N,N-Dimethylacetamide
N,N-二甲基乙酰胺
99.8%, water ≤ 50 ppm
Dimethyl carbonate
碳酸二甲酯
99.5%, water ≤ 20 ppm
N,N-Dimethylformamide
N,N-二甲基甲酰胺
99.8%, water ≤ 50 ppm
Dimethyl sulfide
甲硫醚
99%, water ≤ 30 ppm
Dimethyl sulfoxide
二甲基亞砜
99.7%, water ≤ 50 ppm
1,4-Dioxane
1,4-二氧六環(huán)
99.8%, stabilized with BHT, water ≤ 50 ppm
1,3-Dioxolane
1,3-二氧戊環(huán)
99.8%, stabilized with BHT, water ≤ 30 ppm
Dodecane
正十二烷
99%, water ≤ 30 ppm
Ethanol
乙醇
99.5%, water ≤ 50 ppm
Ethyl acetate
乙酸乙酯
99.5%, water ≤ 50 ppm
n-Heptane
正庚烷
99%, water ≤ 10 ppm
n-Hexane
正己烷
97.5%, water ≤ 50 ppm
Hexanol
正己醇
99%, water ≤ 50 ppm
Isoamyl acetate
乙酸異戊酯
99%, water ≤ 50 ppm
Isopropanol
異丙醇
99.5%, water ≤ 50 ppm
Methanol
甲醇
99.9%, water ≤ 30 ppm
2-Methoxyethanol
2-甲氧基乙醇
99%, water ≤ 50 ppm
Methyl acetate
乙酸甲酯
99%, water ≤ 30 ppm
3-Methyl-1-butanol
3-甲基-1-丁醇
99%, water ≤ 30 ppm
Methyl tert-butyl ether
甲基叔丁基醚
99.8%, water ≤ 30 ppm
Methylcyclohexane
甲基環(huán)已烷
99%, water ≤ 20 ppm
Methyl formate
甲酸甲酯
99%, water ≤ 50 ppm
2-Methyl-1-propanol
2-甲基-1-丙醇
99.5%, water ≤ 30 ppm
1-Methyl-2-pyrrolidinone
1-甲基-2-吡咯烷酮
99.5%, water ≤ 50 ppm
2-Methyltetrahydrofuran
2-甲基四氫呋喃
99%, water ≤ 20 ppm
n-Nonane
正壬烷
99%, water ≤ 50 ppm
1-Octanol
1-辛醇
99%, water ≤ 30 ppm
n-Pentane
正戊烷
99%, water ≤ 10 ppm
Petroleum ether, boiling range 60 - 90℃
石油醚
98%, water ≤ 50 ppm
1-Propanol
1-丙醇
99.7%, water ≤ 50 ppm
Propylene carbonate
碳酸丙烯酯
99.5%, water ≤ 50 ppm
Pyridine
吡啶
99.5%, water ≤ 30 ppm
Tetrachloroethylene
四氯乙烯
99%, water ≤ 50 ppm
Tetrahydrofuran
四氫呋喃
99.9%, stabilized with BHT, water ≤ 50 ppm
Triethyl orthoformate
原甲酸三乙酯
98%, water ≤ 30 ppm
2,2,4-Trimethylpentane
2,2,4-三甲基戊烷
99.8%, water ≤ 30 ppm
Trichloroethylene
三氯乙烯
99%, stabilized, water ≤ 20 ppm
o-Xylene
鄰二甲苯
99%, water ≤ 30 ppm
m-Xylene
間二甲苯
99%, water ≤ 20 ppm
Xylenes
二甲苯
99%, mixed isomers, water ≤ 50 ppm

J&K鋼瓶使用說明書

★ 本鋼瓶為指定溶劑專用鋼瓶,只可盛裝鋼瓶標簽所示產品,不得擅自挪作它用。
★ 本鋼瓶為壓力容器,其儲存和使用場所的環(huán)境溫度不得超過45℃;在裝卸和使用的過程中要注意輕拿輕放,不 得用力裝卸,跌落,撞擊等;本鋼瓶如盛裝強還原性物質時,不得與其它強氧化性物質(例如氧氣等)和腐蝕性物質(例如各種酸類等)混裝混放;不得橫放或倒置。
★ 本鋼瓶為百靈威科技有限公司專門定制的產品,鋼瓶上有百靈威科技有限公司的專用標記。退還鋼瓶時不得以其它外形相似的鋼瓶混雜。
★ 每只鋼瓶配套的有Y型三通角閥一只,角閥外有兩只配套的防漏悶蓋。使用完畢后,應將角閥關閉嚴密之外,還應將外部連接處擦拭干凈(注意:不得使用濕抹布擦拭),將防漏悶蓋裝上并擰緊。
★ 本鋼瓶盛裝的物品為水氧敏感產品,應注意避免物料和水氧接觸。如果瓶內的壓力不足時,可以使用高純氮氣從氣相口加壓。連接管道時要注意首先一定要把管道吹凈、吹干。
★ 本鋼瓶的氣相和液相接口按照下圖識別:
★ 主要技術規(guī)格說明:
公稱容積:12 L
公稱工作壓力: 2.0 Mpa
內直徑: 230 mm
主體設計壁厚: 2.3 mm
總長度: 464 mm
水壓試驗壓力: 4.5 Mpa
氣密性試驗壓力:3.0 Mpa
充裝介質:R-22
最大充裝量:12.2 Kg
鋼瓶理論凈重:8.5Kg(不包括可拆件)
主體鋼板牌號:HP295
材料標準代號:GB 6653-94且,符合GB 5100的規(guī)定
材料化學成分規(guī)定值(%):C≤0.22; Si≤0.45; Mn≤1.60; P≤0.04; S≤0.04; S+P≤0.07
材料強度規(guī)定值:δb ≥440 Mpa δs ≥295 Mpa
鋼瓶熱處理方法:
整體消除應力熱處理
加熱溫度:600±20℃
保溫時間:15min
冷卻方式:爐冷+空冷

J&KSeal 無水無氧包裝

J&KSeal高品質無水無氧包裝具有創(chuàng)新的螺紋密封蓋設計、七孔抽取面設計及PTFE及硅樹脂雙層隔膜瓶墊設計,可最大程度保證產品的品質。對空氣和潮濕敏感類試劑產品,如格氏試劑、鋰類試劑、超干溶劑等,百靈威均采用J&KSeal專業(yè)無水無氧包裝,與市場上的其它包裝相比,J&KSeal包裝可表現(xiàn)出最優(yōu)異的性能:
★ 黃色安全手扣確保產品未被開啟,瓶蓋內側襯墊保證密封性,防止產品污染。
★ 密封螺紋結構設計,蓋與瓶身多重螺紋密合,最大程度保證密封性。
★ 獨特的七孔抽取面可避免同一地方多次穿刺,減小變形的危險性,并具有更好的再次密封性。
★ 具有大面積抽取優(yōu)勢,比其它同類包裝的抽取面積大15倍,方便針頭穿入。
★ 雙層隔膜瓶墊厚度是其它同類包裝的兩倍,保證針刺后再次密封,同時有效降低隔膜發(fā)生膨脹變形幾率。
★ 雙層隔膜瓶墊由PTFE層與硅樹脂材質制成,注射器針頭穿刺應力小,最大程度降低穿刺取樣時發(fā)生意外幾率。
★ 注射器及擰蓋兩種方法取樣,滿足客戶不同用量的需求。
 

 

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